Figure 4-6. HPLC/APCI-MS chromatogram of the randomized mixture of OOO (D9-C18:1) and EEE (D9t-C18:1) using Ag-HPLC with three ChromSpher Lipids columns with a total length of 75 cm, flow rate 1 mL/min, column temperature 25oC, gradient of hexanee2 propanoleacetonitrile. Ag-HPLC, silver-ion high performance liquid chromatography; APCI, atmospheric pressure chemical ionization; MS, mass spectrometry.
Reprinted with permission from Holcapek, M., Velnska´, H., Lı´sa, M., Cesla, P., 2009. Orthogonality of silver-ion and non-aqueous reversed-phase HPLC/MS in the analysis of complex natural mixtures of triacylglycerols. J. Sep. Sci. 32, 3672-3680.
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