Line-shape of chromatograms showed by isomeric IA and IB species that undergo interconversion during elution through the chromatographic column.
Thermodynamic cycle involved during dynamic chromatography experiments (for the meaning of symbols, see text).
Calculation of free energy activation barriers and their enthalpic and entropic contributions.
Activation entropies (deltaS, e.u.) and free energies (deltaG, kcal/mol) of conformational and configurational isomerizations calculated by DHPLC and DHRGC.
Optimal range of applicability of dynamic chromatography [including gas chromatography (GC), high-performance liquid chromatography (HPLC), and ultra-high performance liquid chromatography (UHPLC)] and dynamic nuclear magnetic resonance (DNMR) techniques in the determination of activation barriers for isomerization processes.
Ultra-fast enantioresolution of N-(1-(naphthalen-5 yl) ethyl)-1-naphthamide on the 1.9 um DACH-DNB CSP packed into a stainless-steel (50 x 4.1 mm I.D.) column.
Van Deemter plot for chiral and achiral compounds on Whelk-O1 chiral stationary phases. (A) 250 x 4.6 mm I.D. column packed with fully-porous particles of 5-um average size. (B) 100 x 4.6 mm I.D. column packed with fully-porous particles of 1.7-um average size. Eluent: hexane/dichloromethane 8:2 (v/v) + 3% methanol.
The Handbook of Advanced Chromatography /Mass Spectrometry Techniques is a compendium of new and advanced analytical techniques that have been developed in recent years for analysis of all types of molecules in a variety of complex matrices, from foods to fuel to pharmaceuticals and more. Focusing on areas that are becoming widely used or growing rapidly, this is a comprehensive volume that describes both theoretical and practical aspects of advanced methods for analysis. Written by authors who have published the foundational works in the field, the chapters have an emphasis on lipids, but reach a broader audience by including advanced analytical techniques applied to a variety of fields.
Contains both practical and theoretical knowledge, providing core understanding for implementing modern chromatographic and mass spectrometric techniques Presents chapters on the most popular and fastest-growing new techniques being implemented in diverse areas of research.
The Handbook is intended for upper level undergraduate students and graduate students, researchers, technicians, and scientists.It is also well suited for advanced analytical instrumentation students as well as for analysts seeking additional knowledge or a deeper understanding of familiar techniques.
No. of pages: 520
Copyright: © Academic Press and AOCS Press 2017
Published: September 11th 2017
eBook ISBN: 9780128117330
Paperback ISBN: 9780128117323